Isobutyraldehyde → HCID 68594031, compound
Reaction equation
[CH3:1][C:2]1[CH:13]=[CH:12][C:5]([CH2:6][N:7]2[CH:11]=[N:10][CH:9]=[N:8]2)=[CH:4][CH:3]=1.[CH:14](=[O:18])[CH:15]([CH3:17])[CH3:16]>>[CH3:16][CH:15]([CH3:17])[CH:14]([C:11]1[N:7]([CH2:6][C:5]2[CH:4]=[CH:3][C:2]([CH3:1])=[CH:13][CH:12]=2)[N:8]=[CH:9][N:10]=1)[OH:18]Participants
3
Procedure
2-Methyl-1-[1-(4-methylbenzyl)-1H-1,2,4-triazol-5-yl]propan-1-ol was synthesized in a manner similar to that of procedure 21 B but using 1-(4-methylbenzyl)-1H-1,2,4-triazole and isobutyraldehyde as the starting materials. The product was isolated as a white solid in 66% yield.
Workup
- customThe product was isolated as a white solid in 66% yield
Sources & evidence
- ORD record
- ord-7cbd94594ab74ceab87fba8243af7d26
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07399778B2
Reaction notes
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