HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22939353, compound → HCID 59750359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22939353 | HCID 22939353 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 59750359 | HCID 59750359 | 69% |
Reaction Steps
2-(6-(Benzyloxy)-2-pyridyl)-4H-1,3-benzothiazine-4-one (0.15 g, 0.43 mmol) was dissolved in trifluoroacetic acid (10 ml), and the mixture was stirred at room temperature for 15 hrs. The solvent was evaporated, and the residue was recrystallized from chloroform-hexane to give the titled compound (0.07 g, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399759B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-92b954082ba34b7cac39b11d24dfaca4 |
| Source note | uspto-grants-2008_07 |