HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 22041442, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 12045143 | HCID 12045143 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22041442 | HCID 22041442 | 101.9% |
Reaction Steps
Into 30 mL of methanol was dissolved 290 mg of Compound 23, followed by addition of 77 mg of sodium methoxide. After 8 hours of stirring at room temperature, ether was added and the precipitated crystals were collected by filtration and washed with ether to obtain 300 mg of the title compound as colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399781B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-c497f0ec0edd4b038063397a3a37065f |
| Source note | uspto-grants-2008_07 |