HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 86658288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 86658289 | HCID 86658289 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | MeOH tetrahydrofuran | HCID 21899815 | — |
| Product | HCID 86658288 | HCID 86658288 | 90% |
Reaction Steps
Peracetate 95 (190 mg) was dissolved in THF/MeOH (1:1). NaOMe in MeOH (11M, 20 μL) was added and the solution was stirred at room temperature for 3 hours. The solution was neutralised with H+ resin, filtered and the solvent evaporated to give 125 mg (90%) of the off-white solid product which was reacted on without further purification or characterisation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08828952B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-b6602bf2aa9b4b81b5c93438824b0c39 |
| Source note | uspto-grants-2014_09 |