HCID 822459, compound → HCID 136342130, compound

Participants

Reaction Steps

The title compound was prepared as described for Example 82 using 5-cyanooxindole and 1-[(6-chloropyridin-3-yl)sulfonyl]-4-ethylpiperazine. Yield: 4% of the title compound as a yellow solid: 1H NMR (DMSO-d6, 400 MHz) δ 11.15 (br s, 1 H), 10.75 (br s, 1 H), 8.56 (br s, 1 H), 8.04 (s, 1 H), 7.93-7.82 (m, 1 H), 7.73 (dd, J=9, 2 Hz, 1 H), 7.41 (dd, J=8, 1 Hz, 1 H), 7.05 (d, J=8 Hz, 1 H), 3.83-3.69 (m, 2 H), 3.69-3.42 (m, 2 H), 3.18-2.92 (m, 6 H), 1.20 (t, J=7.2 Hz, 3 H); MS (ES) m/z 412 (M++1).

Provenance & Evidence