tert-Butyldimethylsilyl chloride → Tert-butyl(3-ethoxy-2,2-dimethylpropoxy)dimethylsilane
Reaction equation
[CH3:1][C:2]([CH3:9])([CH2:5][O:6][CH2:7][CH3:8])[CH2:3][OH:4].[Si:10](Cl)([C:13]([CH3:16])([CH3:15])[CH3:14])([CH3:12])[CH3:11]>>[CH3:1][C:2]([CH3:9])([CH2:3][O:4][Si:10]([C:13]([CH3:16])([CH3:15])[CH3:14])([CH3:12])[CH3:11])[CH2:5][O:6][CH2:7][CH3:8]Participants
3
Procedure
According to the procedure as described in Example 3,2,2-dimethyl-1-ethoxy-3-[(tert-butyldimethylsilyl)oxy]propane was prepared from intermediate 2,2-dimethyl-3-ethoxy-1-propanol and reagent tert-butyidimethylsilyl chloride.
Sources & evidence
- ORD record
- ord-9a9448b7764049e9bfb09776de261208
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07399812B2
Reaction notes
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