tert-Butyldimethylsilyl chloride → HCID 86248050, compound
Reaction equation
[CH2:1]([C:5]([CH2:11][CH2:12][CH2:13][CH3:14])([CH2:8][O:9][CH3:10])[CH2:6][OH:7])[CH2:2][CH2:3][CH3:4].[Si:15](Cl)([C:18]([CH3:21])([CH3:20])[CH3:19])([CH3:17])[CH3:16]>>[CH2:1]([C:5]([CH2:11][CH2:12][CH2:13][CH3:14])([CH2:6][O:7][Si:15]([C:18]([CH3:21])([CH3:20])[CH3:19])([CH3:17])[CH3:16])[CH2:8][O:9][CH3:10])[CH2:2][CH2:3][CH3:4]Participants
3
Procedure
According to the procedure as described in Example 8,2,2-di-n-butyl-1-methoxy-3-[(tert-butyldimethylsilyl)oxy]propane was prepared from intermediate 2,2-di-n-butyl-3-methoxy-1-propanol and reagent tert-butyidimethylsilyl chloride.
Sources & evidence
- ORD record
- ord-67ed394cc95e489a8ba0af0e43a635e1
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07399812B2
Reaction notes
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