HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68518345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 59751437 | HCID 59751437 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68518345 | HCID 68518345 | 100% |
Reaction Steps
Dissolve the compound of Example 7 (99 mg, 0.15 mmol) in dichloromethane (3 mL) and add 2M HCl in ether (400 μL, 0.8 mmol). Remove the solvent in vacuo to yield 111 mg of the title compound (100%): mass spectrum (ion spray): m/z=640.3 (M+H—HCl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07399867B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-a0cddba28ee04dadad88d50da10fb51b |
| Source note | uspto-grants-2008_07 |