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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 748876Generated: October 29, 2026

Hydrochloric Acid → HCID 68518345, compound

https://huagongshe.com/reaction/748876

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 59751437HCID 59751437—
SolventDichloromethaneHCID 6344—
ProductHCID 68518345HCID 68518345100%

Reaction Steps

Dissolve the compound of Example 7 (99 mg, 0.15 mmol) in dichloromethane (3 mL) and add 2M HCl in ether (400 μL, 0.8 mmol). Remove the solvent in vacuo to yield 111 mg of the title compound (100%): mass spectrum (ion spray): m/z=640.3 (M+H—HCl).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07399867B2
Source datasetuspto-grants-2008_07
ORD IDord-a0cddba28ee04dadad88d50da10fb51b
Source noteuspto-grants-2008_07