HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoroethyl bromide → HCID 22235038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoroethyl bromide | HCID 12982 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 12425844 | HCID 12425844 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22235038 | HCID 22235038 | 50.7% |
Reaction Steps
Using 0.37 g of (4-fluorobenzyl)malononitrile, 5 ml of N,N-dimethylformamide, 0.12 g of sodium hydride (60% in oil), and 0.25 g of 1-bromo-2-fluoroethane, and according to the process described in the Production Example 1, there was obtained 0.22 g of 2-(4-fluorobenzyl)-2-(2-fluoroethyl)malononitrile (the present compound (59)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402691B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-cac91859c7f54567b78c2a27764b36c1 |
| Source note | uspto-grants-2008_07 |