HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22235063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 22234971 | HCID 22234971 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22235063 | HCID 22235063 | 90% |
Reaction Steps
Using 1.42 g of (2,4,6-trifluorobenzyliden)malononitrile, 50 ml of ethanol and 0.08 g of sodium borohydride, and according to the process described in the Reference Production Example 3, there was obtained 1.29 g of (2,4,6-trifluorobenzyl)malononitrile (the intermediate (21)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402691B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-c5b0630c08f9443ab7cdcc6e2ad98906 |
| Source note | uspto-grants-2008_07 |