HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 53325849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | p-Chloro-beta-nitrostyrene | HCID 95339 | — |
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Solvent | Toluene ethanol | HCID 21863594 | — |
| Product | HCID 53325849 | HCID 53325849 | — |
Reaction Steps
The title compound (1.19 g) was prepared from 1.55 g of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester, 850 μL of benzylamine, and 1.43 g of 1-chloro-4-(2-nitro-vinyl)-benzene, using a 1:1 mixture of EtOH/toluene as the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402680B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-9e105893f7da4d009949eadedbe9765f |
| Source note | uspto-grants-2008_07 |