HuagongsheHuagongshe Chemistry Print Report · For research reference only
Beta-Nitrostyrene → HCID 53323185, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Beta-Nitrostyrene | HCID 7626 | — |
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | HCID 67269021 | HCID 67269021 | — |
| Solvent | Benzylamine | HCID 7504 | — |
| Product | HCID 53323185 | HCID 53323185 | — |
Reaction Steps
1-Benzyl-3-phenyl-1,4,6,7-tetrahydro-pyrrolo[3,2-c]pyridine-5-carboxylic acid tert-butyl ester. The desired compound (380.7 mg) was prepared from 0.51 g of 4-oxo-piperidine-1-carboxylic acid tert-butyl ester, 280 μL of benzylamine, and 0.39 g of (2-nitro-vinyl)-benzene as in Example 1, Step A. MS (ESI): exact mass calculated for C25H28N2O2, 388.22; found, m/z 389.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402680B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-5cb2fa6cbe8b45b9ba20510ed2117786 |
| Source note | uspto-grants-2008_07 |