1,4-Dioxane hydrochloride → HCID 69001602, compound

Participants

Reaction Conditions

Reaction Steps

To the product from step 5 (0.60 g, 1.42 mmol) was added a 1:1 mixture of concentrated HCl/dioxane (28 mL). The resulting solution was stirred at 60° C. for 4 h. The solvent was removed in vacuo. The crude product was triturated with ether and dried under reduced pressure to afford the title compound (0.49 g, 52%) as a white solid.

Provenance & Evidence