4-Methylsulfonylbenzylamine → HCID 69155595, compound

HRID 750120Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[O:10])[O:8][C:6](=O)[C:5]2=[CH:11][CH:12]=1.[CH3:13][S:14]([C:17]1[CH:24]=[CH:23][C:20]([CH2:21][NH2:22])=[CH:19][CH:18]=1)(=[O:16])=[O:15]>>[CH3:6][O:8][C:9]([C:4]1[N:22]([CH2:21][C:20]2[CH:23]=[CH:24][C:17]([S:14]([CH3:13])(=[O:15])=[O:16])=[CH:18][CH:19]=2)[C:6](=[O:8])[C:5]2[C:4]([C:9]=1[OH:10])=[CH:3][C:2]([Cl:1])=[CH:12][CH:11]=2)=[O:10]

Participants

Reactant 2

HCID 574214-Methylsulfonylbenzylamine

HCID 670444-Chlorophthalic anhydride

Product 1

HCID 69155595HCID 69155595, compound

Procedure

The present compound was synthesized according to the method shown in Reference Example 8 and using 4-chloro phthalic anhydride and 4-(methanesulfonyl)benzylamine.

Workup

customThe present compound was synthesized

Sources & evidence

ORD record: ord-86a42318afba42e8ad6696f49fe802b9
Source dataset: uspto-grants-2008_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07402595B2

Reaction notes

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