Phenoxyethanol → HCID 69157381, compound

HRID 750191Notes

Reaction equation

HRID 750191 reaction equation
[CH2:1]([O:8][C:9]([N:11]([CH3:33])[N:12]1[C:21]([C:22]([OH:24])=[O:23])=[C:20]([C:25]2[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=2)[C:19]2[C:14](=[CH:15][CH:16]=[C:17]([Cl:31])[CH:18]=2)[C:13]1=[O:32])=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[O:34]([CH2:41][CH2:42]O)[C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1>>[O:34]([CH2:41][CH2:42][O:23][C:22]([C:21]1[N:12]([N:11]([C:9]([O:8][CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[O:10])[CH3:33])[C:13](=[O:32])[C:14]2[C:19]([C:20]=1[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1)=[CH:18][C:17]([Cl:31])=[CH:16][CH:15]=2)=[O:24])[C:35]1[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1

Participants

3

Reactant 2

HCID 31236PhenoxyethanolHCID 691557392-[(benzyloxycarbonyl)(methyl)amino]-6-chloro-1-oxo-4-phenyl-1,2-dihydroisoquinoline-3-carboxylic Acid

Product 1

HCID 69157381HCID 69157381, compound

Procedure

The present compound was synthesized by a method similar to that in Example 200 using 2-[(benzyloxycarbonyl)(methyl)amino]-6-chloro-1-oxo-4-phenyl-1,2-dihydroisoquinoline-3-carboxylic acid (150 mg) and 2-phenoxyethanol. A colorless powder (78 mg).

Sources & evidence

ORD record
ord-2981b87b907d45b4903cf701aee8d058
Source dataset
uspto-grants-2008_07
Patent number
US07402595B2

Reaction notes

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