3-Methylbutanal → HCID 69156456, compound

HRID 750196Notes

Reaction equation

HRID 750196 reaction equation
[CH3:1][O:2][C:3]([C:5]1[N:6]([NH2:23])[C:7](=[O:22])[C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][CH:9]=2)=[O:4].[CH:24](=O)[CH2:25][CH:26]([CH3:28])[CH3:27]>>[CH3:1][O:2][C:3]([C:5]1[N:6]([N:23]=[CH:24][CH2:25][CH:26]([CH3:28])[CH3:27])[C:7](=[O:22])[C:8]2[C:13]([C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[CH:12][C:11]([Cl:21])=[CH:10][CH:9]=2)=[O:4]

Participants

3

Reactant 2

HCID 115523-MethylbutanalHCID 69156379HCID 69156379, compound

Product 1

HCID 69156456HCID 69156456, compound

Procedure

The present compound was synthesized by a method similar to that in Example 210 and using 2-amino-6-chloro-1-oxo-4-phenyl-1,2-dihydroisoquinoline-3-carboxylic acid methyl ester (210 mg) and isovaleraldehyde. A colorless powder (95 mg).

Workup

  1. customThe present compound was synthesized by a method similar to that in Example 210

Sources & evidence

ORD record
ord-9f23879745164119b3b7df10df64c439
Source dataset
uspto-grants-2008_07
Patent number
US07402595B2

Reaction notes

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