Benzo-1,3-dioxole-5-methylamine → HCID 23060867, compound

HRID 750205Notes

Reaction equation

HRID 750205 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[C:8](=[O:12])O[C:6]([C:13]([OH:15])=[O:14])=[C:5]2[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1.[CH2:22]([NH2:32])[C:23]1[CH:31]=[CH:30][C:29]2[O:28][CH2:27][O:26][C:25]=2[CH:24]=1>>[O:28]1[C:29]2[CH:30]=[CH:31][C:23]([CH2:22][N:32]3[C:6]([C:13]([OH:15])=[O:14])=[C:5]([C:16]4[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=4)[C:4]4[C:9](=[CH:10][CH:11]=[C:2]([Cl:1])[CH:3]=4)[C:8]3=[O:12])=[CH:24][C:25]=2[O:26][CH2:27]1

Participants

3

Reactant 2

HCID 75799Benzo-1,3-dioxole-5-methylamineHCID 103800926-chloro-4-phenylisocoumarin-3-carboxylic Acid

Product 1

HCID 23060867HCID 23060867, compound

Procedure

The present compound was synthesized by a method similar to that in Example 226 and using 6-chloro-1-oxo-4-phenyl-1H-isochromen-3-carboxylic acid (400 mg) and piperonylamine.

Workup

  1. customThe present compound was synthesized by a method similar to that in Example 226

Sources & evidence

ORD record
ord-bfa254db90db49138f9b72adea792ed0
Source dataset
uspto-grants-2008_07
Patent number
US07402595B2

Reaction notes

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