HuagongsheHuagongshe Chemistry Print Report · For research reference only
THF diisopropyl ether → 3-acetyl-6-bromo-2-(4-methanesulfonylbenzyl)-4-phenyl-2H-isoquinolin-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | THF diisopropyl ether | HCID 21940044 | — |
| Reactant | 6-bromo-3-(1-hydroxyethyl)-2-(4-methanesulfonylbenzyl)-4-phenyl-2H-isoquinolin-1-one | HCID 23060925 | — |
| Product | 3-acetyl-6-bromo-2-(4-methanesulfonylbenzyl)-4-phenyl-2H-isoquinolin-1-one | HCID 23060654 | — |
Reaction Steps
In the same manner as in Example 311, the title compound was synthesized using 6-bromo-3-(1-hydroxyethyl)-2-(4-methanesulfonylbenzyl)-4-phenyl-2H-isoquinolin-1-one. Crystals (THF-diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07402595B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-8c2f80ef00c84fcc81ed5a58ca12bbd8 |
| Source note | uspto-grants-2008_07 |