2-Benzoyl-4-chlorobenzoic acid → HCID 69156949, compound
Reaction equation
Cl.[OH:2][CH:3]([CH2:17][CH2:18][CH2:19][CH3:20])[CH2:4][NH:5][CH2:6][C:7]1[CH:12]=[CH:11][C:10]([S:13]([NH2:16])(=[O:15])=[O:14])=[CH:9][CH:8]=1.[C:21]([C:29]1[CH:37]=[C:36]([Cl:38])[CH:35]=[CH:34][C:30]=1[C:31](O)=[O:32])(=O)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1>>[Cl:38][C:36]1[CH:37]=[C:29]2[C:30](=[CH:34][CH:35]=1)[C:31](=[O:32])[N:5]([CH2:6][C:7]1[CH:8]=[CH:9][C:10]([S:13]([NH2:16])(=[O:14])=[O:15])=[CH:11][CH:12]=1)[C:4]([C:3](=[O:2])[CH2:17][CH2:18][CH2:19][CH3:20])=[C:21]2[C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1Participants
3
Procedure
In the same manner as in Example 452, Step 2, the title compound was synthesized from 4-[(2-hydroxyhexylamino)methyl]benzenesulfonamide hydrochloride and 2-benzoyl-4-chlorobenzoic acid.
Sources & evidence
- ORD record
- ord-dd51894a251e40479df91dedf8ce631f
- Source dataset
- uspto-grants-2008_07
- Patent number
- US07402595B2
Reaction notes
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