N,N-Diethyl-1,4-butanediamine → HCID 10457666, compound

HRID 750620Notes

Reaction equation

HRID 750620 reaction equation
C1(O[C:8](=[O:30])[NH:9][C:10]2[S:14][N:13]=[C:12]([O:15][CH2:16][C:17]3[C:22]([F:23])=[CH:21][C:20]([CH3:24])=[C:19]([Cl:25])[C:18]=3[F:26])[C:11]=2[C:27](=[O:29])[NH2:28])C=CC=CC=1.[CH2:31]([N:33]([CH2:39]C)[CH2:34][CH2:35][CH2:36][CH2:37][NH2:38])C>>[Cl:25][C:19]1[C:18]([F:26])=[C:17]([C:22]([F:23])=[CH:21][C:20]=1[CH3:24])[CH2:16][O:15][C:12]1[C:11]([C:27]([NH2:28])=[O:29])=[C:10]([NH:9][C:8]([NH:38][CH2:37][CH2:36][CH2:35][CH2:34][N:33]([CH3:39])[CH3:31])=[O:30])[S:14][N:13]=1

Participants

3

Reactant 2

HCID 117976N,N-Diethyl-1,4-butanediamineHCID 53759174HCID 53759174, compound

Product 1

HCID 10457666HCID 10457666, compound

Procedure

The title compound was prepared [4-carbamoyl-3-(3-chloro-2,6-difluoro-4-methyl-benzyloxy)-isothiazol-5-yl]-carbamic acid phenyl ester and N,N-diethyl-butane-1,4-diamine by the procedure analogous to Example 1. MS (APCl, m/z): 476 [M+H]+.

Sources & evidence

ORD record
ord-1908cf747a884c22a7956a9b4cb51e2d
Source dataset
uspto-grants-2008_07
Patent number
US07405218B2

Reaction notes

Loading…