HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorophenol → HCID 59753906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorophenol | HCID 9743 | — |
| Reactant | HCID 69198607 | HCID 69198607 | — |
| Product | HCID 59753906 | HCID 59753906 | — |
Reaction Steps
2-Methylsulfonyl-4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)pyrimidine from Reference Example 3 was reacted with 3-fluorophenol according to the procedure described in Example 74 to afford 2-(3-fluorophenyloxy)-4-(2,4-dichlorophenyl)-5-(4-chlorophenyl)pyrimidine: HPLC/MS: m/e=445 (M++1); Rt=4.50 min; 1H-NMR 400 MHz (CDCl3): δ 7.05. (m, 3H), 7.21-7.30 (m, 6H), 7.38-7.42 (m, 2H), 8.60 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405221B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-b13c7d48891648e9a4be92d9512b179c |
| Source note | uspto-grants-2008_07 |