HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-2-methylpropionyl bromide → 11-Mercaptoundecyl 2-Bromo-2-methylpropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-2-methylpropionyl bromide | HCID 88685 | — |
| Reactant | 11-Mercaptoundecanol | HCID 261824 | — |
| Product | 11-Mercaptoundecyl 2-Bromo-2-methylpropanoate | HCID 57539288 | — |
Reaction Steps
Mercaptoundecyl bromoisobutyrate was synthesized through the reaction of bromoisobutyryl bromide and 11-mercapto-1-undecanol using a method published previously. 1H NMR (300 MHz, CDCl3): 4.15 (t, J=6.9 Hz, 2H, OCH2), 2.51 (q, J=7.5 Hz, 2H, SCH2), 1.92 (s, 6H, CH3), 1.57-1.72 (m, 4H, CH2), and 1.24-1.40 (m, 16H, CH2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08835144B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-acb88dfe21004e37bae13606ba9b6b2c |
| Source note | uspto-grants-2014_09 |