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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 75086Generated: October 26, 2026

2-Bromo-2-methylpropionyl bromide → 11-Mercaptoundecyl 2-Bromo-2-methylpropanoate

https://huagongshe.com/reaction/75086

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Bromo-2-methylpropionyl bromideHCID 88685—
Reactant11-MercaptoundecanolHCID 261824—
Product11-Mercaptoundecyl 2-Bromo-2-methylpropanoateHCID 57539288—

Reaction Steps

Mercaptoundecyl bromoisobutyrate was synthesized through the reaction of bromoisobutyryl bromide and 11-mercapto-1-undecanol using a method published previously. 1H NMR (300 MHz, CDCl3): 4.15 (t, J=6.9 Hz, 2H, OCH2), 2.51 (q, J=7.5 Hz, 2H, SCH2), 1.92 (s, 6H, CH3), 1.57-1.72 (m, 4H, CH2), and 1.24-1.40 (m, 16H, CH2).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08835144B2
Source datasetuspto-grants-2014_09
ORD IDord-acb88dfe21004e37bae13606ba9b6b2c
Source noteuspto-grants-2014_09