Ethanimidic acid, ethyl ester, hydrochloride (1:1) → 3,5-Difluoro-benzoic acid-(1-imino-ethyl)-hydrazide

HRID 750887Notes

Reaction equation

HRID 750887 reaction equation
Cl.C(O[C:5](=[NH:7])[CH3:6])C.[F:8][C:9]1[CH:10]=[C:11]([CH:16]=[C:17]([F:19])[CH:18]=1)[C:12]([NH:14][NH2:15])=[O:13]>>[NH:7]=[C:5]([N:14]([C:12](=[O:13])[C:11]1[CH:10]=[C:9]([F:8])[CH:18]=[C:17]([F:19])[CH:16]=1)[NH2:15])[CH3:6]

Participants

3

Reactant 2

HCID 2724290Ethanimidic acid, ethyl ester, hydrochloride (1:1)HCID 27369243,5-Difluorobenzohydrazide

Product 1

HCID 684952773,5-Difluoro-benzoic acid-(1-imino-ethyl)-hydrazide

Procedure

The compound is obtained analogously to the method described for intermediate product 1a) from 4.91 g (40 mmol) ethylacetimidate hydrochloride and 3.80 g (22 mmol) 3,5 difluoro-benzoic acid hydrazide.

Workup

  1. customThe compound is obtained analogously to the method

Sources & evidence

ORD record
ord-112bdacfa2c34a1ebcaccbed12b2cbce
Source dataset
uspto-grants-2008_07
Patent number
US07405232B2

Reaction notes

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