反应详情

A large excess of thionyl chloride was added to 10 g of the p-octyloxybenzoic acid prepared in (1), and the mixture was refluxed for 5 hours. Excessive thionyl chloride was distilled off to give a crude end compound.

1. temperaturethe mixture was refluxed for 5 hours
2. distillationExcessive thionyl chloride was distilled off
3. customto give a crude end compound