HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-1H-indole-3-carbaldehyde → HCID 86035906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-1H-indole-3-carbaldehyde | HCID 314791 | — |
| Reactant | (3-Bromophenyl)boronic acid | HCID 2734318 | — |
| Product | HCID 86035906 | HCID 86035906 | 87% |
Reaction Steps
2-Chloro-1H-indole-3-carboxaldehyde is reacted with 3-bromophenylboronic acid as described in Step 1 of Example 29 to afford 1-(3-bromophenyl)-2-chloro-1H-indole-3-carboxaldehyde (87% yield) as a cream solid. ESI/MS 334 (M), 375 [(M+2+CH3CN) adduct]; RT 3.59 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405300B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-53b66342713a45ae9fd7669cee707ebf |
| Source note | uspto-grants-2008_07 |