HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-1H-indole-3-carbaldehyde → HCID 86035924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-1H-indole-3-carbaldehyde | HCID 314791 | — |
| Reactant | 4-Phenoxyphenylboronic acid | HCID 2734377 | — |
| Product | HCID 86035924 | HCID 86035924 | 34% |
Reaction Steps
2-Chloro-1H-indole-3-carboxaldehyde is reacted with 4-phenoxyphenylboronic acid as described in Step 1 of Example 29 to afford 2-chloro-1-(4-phenoxyphenyl)-1H-indole-3-carboxaldehyde (34% yield) as a cream solid. ESI/MS 348 (M+H), 389 [(M+1+CH3CN) adduct], RT 3.74 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405300B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-e3e175425ada46c3be03020f9410e158 |
| Source note | uspto-grants-2008_07 |