HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-1H-indole-3-carbaldehyde → HCID 86035939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-1H-indole-3-carbaldehyde | HCID 314791 | — |
| Reactant | [3-(Hydroxymethyl)phenyl]boronic acid | HCID 2734662 | — |
| Product | HCID 86035939 | HCID 86035939 | 17% |
Reaction Steps
2-Chloro-1H-indole-3-carboxaldehyde is reacted with 3-(hydroxymethyl)-phenylboronic acid as described in Step 1 of Example 29 to afford 2-chloro-1-(3-hydroxymethylphenyl)-1H-indole-3-carboxaldehyde (17% yield) as a pink solid. ESI/MS 286 (M+H); RT 2.85 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405300B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-a4b0c6237d44472d9fa3c381f0a19a21 |
| Source note | uspto-grants-2008_07 |