HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59753698, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Boc-4-(aminomethyl)piperidine | HCID 736817 | — |
| Reactant | HCID 86601768 | HCID 86601768 | — |
| Product | HCID 59753698 | HCID 59753698 | — |
Reaction Steps
Prepared according to EXAMPLE 191 from 5-chloro-1H-pyrrolo[2,3-c]pyridine-2-carboxylic acid [1-(S)-(4-fluorobenzyl)-2-(4-{[methyl-(2-nitrobenzenesulfonyl)amino]methyl}piperidin-1-yl)-2-oxoethyl]amide (synthesised according to Preparations 73-76 from the 4-aminomethylpiperidine-1-carboxylic acid tert-butyl ester starting material). m/z (ES+) free base=472.33 [M+H]+; RT=2.80 min. m/z (ES+) HCl salt=430.43 [M+H]+; RT=2.72 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07405210B2 |
| Source dataset | uspto-grants-2008_07 |
| ORD ID | ord-329e4e87041b47809ec23bb74a0c3805 |
| Source note | uspto-grants-2008_07 |