HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethanol → 2-(Pyridin-3-yloxy)ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethanol | HCID 34 | — |
| Reactant | 3-Hydroxypyridine | HCID 7971 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(Pyridin-3-yloxy)ethan-1-ol | HCID 21908997 | — |
Reaction Steps
The yield of the title compound according to D1, starting from 3-hydroxypyridine, 2-chloroethanol and K2CO3 in DMF was 19%. The title compound has also been prepared according to EP 0 286 242 A2 starting from methyl [(3-pyridinyl)oxy]acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08835439B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-b440f9e1831244a0b541a4df6290b27d |
| Source note | uspto-grants-2014_09 |