Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 76090Erstellt: 25. Oktober 2026

Propionyl chloride → Bis-benzyloxy benzoic acid

https://huagongshe.com/reaction/76090

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPropionyl chlorideHCID 62324—
EduktMethyl 2,3-bis(benzyloxy)benzoateHCID 10665397—
ProduktBis-benzyloxy benzoic acidHCID 10520703—

Reaktionsschritte

In another embodiment the compounds can be prepared as shown in Scheme III. A nitroaniline (1) can be reacted with propionyl chloride to yield nitro-phenyl-propionamide (2). NaH can then be added to a solution of (2) in anhydrous THF followed by iodomethane to give pure product nitro-phenyl-N-methyl-propionamide (3).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08835464B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-08fba97b67914e08bba8c8f330580161
Quellennotizuspto-grants-2014_09