HRID76181

反应详情

EQUATION

反应方程式

HRID 76181 的结构方程式

PROCEDURE

实验过程

To 0.50 g (3.18 mmol) 2-oxo-pyrollidine-carboxylic acid ethyl ester in 10 mL EtOH are added 5 mL aq. NaOH (1M) solution. The reaction mixture is stirred at r.t. for 3 h. The EtOH is removed in vacuo and the residue is diluted with water and acidified with aq. HCl (2M) solution. The resulting precipitate is filtered and dried.

WORKUP

后处理

  1. customThe EtOH is removed in vacuo
  2. additionthe residue is diluted with water
  3. filtrationThe resulting precipitate is filtered
  4. customdried