HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methoxycarbonyl)bicyclo[2.2.2]octane-1-carboxylic acid → HCID 178441255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methoxycarbonyl)bicyclo[2.2.2]octane-1-carboxylic acid | HCID 11042062 | — |
| Reactant | 2-tert-Butyl-4-butylisothiazol-5(2H)-imine | HCID 66867228 | — |
| Product | HCID 178441255 | HCID 178441255 | — |
Reaction Steps
The product from Example 92B and 4-(methoxycarbonyl)bicyclo[2.2.2]octane-1-carboxylic acid (Oakwood) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.91 (t, J=7.3 Hz, 3H), 1.23-1.36 (m, 2H), 1.58 (s, 9H), 1.58-1.66 (m, 2H), 1.70-1.83 (m, 12 H), 2.61-2.66 (m, 2H), 3.58 (s, 3H), 8.49 (s, 1H). (ESI+) m/z 407 (M+H)+. Anal. calcd. for C22H34N2O3S: C, 64.99; H, 8.43; N, 6.89. Found: C, 64.65; H, 8.24; N, 6.72.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08835475B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-82782e70f799494ebd7bab0ca87e8fd8 |
| Source note | uspto-grants-2014_09 |