HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 68025181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Oxazinone | HCID 21873527 | — |
| Product | HCID 68025181 | HCID 68025181 | 96% |
Reaction Steps
Procedure & NMR Data: 107 mg (2.5 eq, 0.58 mmol) of 4-Nitrobenzoyl chloride was added to a mixture of 37 mg (4 eq, 0.92 mmol) of NaH and 50 mg (0.23 mmol) of oxazinone P2 in THF (10 mL). 81 mg of P7 were obtained, yield 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08835628B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-de68aadbd1514f7a8c8180039b8ede36 |
| Source note | uspto-grants-2014_09 |