Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-bromobutanimide → 4-Bromomethyl-2,5-dimethoxybenzonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 2,5-Dimethoxy-4-methylbenzonitrile | HCID 595738 | — |
| 생성물 | 4-Bromomethyl-2,5-dimethoxybenzonitrile | HCID 58827058 | — |
반응 단계
2,5-Dimethoxy-4-methylbenzonitrile (4.06 g, 21.5 mmol) is brominates with NBS according to Example 1A to give 4-bromomethyl-2,5-dimethoxybenzonitrile. 1H NMR (400 MHz, CDCl3) δ (ppm) 6.95 (s, 1H), 6.91 (s, 1H), 4.43 (s, 2H), 3.84 (s, 3H), 3.80 (s, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835646B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-cee3297a78c8402b94cb6de8ee48ff8d |
| 출처 메모 | uspto-grants-2014_09 |