HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanol → HCID 59255186, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanol | HCID 59255370 | — |
| Katalysator | HCID 178418406 | HCID 178418406 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 59255186 | HCID 59255186 | 83% |
Reaktionsschritte
To a mixture of (4-(5-chloro-furan-2-ylmethyl)-phenyl)-methanol (650 mg, 2.9 mmol) described in Manufacturing Example 62-1-3 and dichloromethane (20 mL) was added manganese dioxide (6.5 g, 75 mmol) at room temperature, which was stirred overnight at room temperature. The reaction mixture was filtered through a Celite pad. The filtrate was evaporated under a reduced pressure to obtain the title compound (530 mg, 83%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08841327B2 |
| Quelldatensatz | uspto-grants-2014_09 |
| ORD ID | ord-e1482f86117b4daf940bdf268d01a279 |
| Quellennotiz | uspto-grants-2014_09 |