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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 77957Erstellt: 26. Oktober 2026

(4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanol → HCID 59255186, Verbindung

https://huagongshe.com/reaction/77957

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt(4-(5-Chloro-furan-2-ylmethyl)-phenyl)-methanolHCID 59255370—
KatalysatorHCID 178418406HCID 178418406—
LösungsmittelDichloromethaneHCID 6344—
ProduktHCID 59255186HCID 5925518683%

Reaktionsschritte

To a mixture of (4-(5-chloro-furan-2-ylmethyl)-phenyl)-methanol (650 mg, 2.9 mmol) described in Manufacturing Example 62-1-3 and dichloromethane (20 mL) was added manganese dioxide (6.5 g, 75 mmol) at room temperature, which was stirred overnight at room temperature. The reaction mixture was filtered through a Celite pad. The filtrate was evaporated under a reduced pressure to obtain the title compound (530 mg, 83%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08841327B2
Quelldatensatzuspto-grants-2014_09
ORD IDord-e1482f86117b4daf940bdf268d01a279
Quellennotizuspto-grants-2014_09