反应详情

温度

60 °C

6-Bromonaphthalene-2-carboxylic acid (25.1 g) was suspended in thionyl chloride (200 mL), stirred at 60° C. for 16 hours and evaporated under vacuum. Solid was dissolved in dichloromethane (50 mL) and evaporated under vacuum, giving 6-bromonaphthalene-2-carbonyl chloride (27.0 g, crude) as a white solid.

1. customevaporated under vacuum
2. dissolutionSolid was dissolved in dichloromethane (50 mL)
3. customevaporated under vacuum