HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → HCID 68783469, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | 6-Aminobenzothiazole | HCID 68288 | — |
| Reactant | 4,4,4-Trifluoro-but-2-enoic acid | HCID 2782431 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 68783469 | HCID 68783469 | 58.6% |
Reaction Steps
Benzothiazol-6-ylamine (1 g, 0.006 mol) was reacted with 4,4,4-trifluoro-but-2-enoic acid (1.39 g, 0.009 mol), benzene-1,4-diol (0.05 g, 0.00046 mol) and toluene (50 mL) to afford the crude product. Purification by column chromatography on silica gel (15% ethyl acetate in hexane) afforded 1.02 g of the product (53.68% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE045173E1 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-64df3c453e2348989f1cbe445a26b772 |
| Source note | uspto-grants-2014_09 |