HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-((Triphenylmethyl)amino)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | Acetaldehyde ammonia | HCID 522583 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 2-((Triphenylmethyl)amino)ethanol | HCID 3125608 | 39% |
Reaction Steps
Triphenylchloromethane (1.00 g, 3.58 mmol) (Wako Pure Chemical Industries, Ltd.) and aminoethanol (2.00 g, 32.7 mmol) were dissolved in acetonitrile (5 mL), and the solution was stirred at room temperature overnight. Water (100 mL) was poured into the reaction solution, and the precipitates were suction-filtered and then dried. The solid product was recrystallized from a mixed solvent of ethanol (Wako Pure Chemical Industries, Ltd.) and water, to thereby obtain the title compound (0.43 g, 39% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846012B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-c8024df5c705406a8ff8676a83e574f1 |
| Source note | uspto-grants-2014_09 |