Benzylamine → HCID 66988089, compound

HRID 80331Notes

Reaction equation

C[N:2]([CH:4]=[C:5]1[CH2:9][CH2:8][CH2:7][C:6]1=[O:10])[CH3:3].C(N)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:3]([NH:2][CH:4]=[C:5]1[CH2:9][CH2:8][CH2:7][C:6]1=[O:10])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

Reactant 2

HCID 7504Benzylamine

HCID 37950082-Dimethylaminomethylenecyclopentanone

Product 1

HCID 66988089HCID 66988089, compoundYield 73.5%

Procedure

Using 2-dimethylaminomethylenecyclopentanone (50 mmol) and benzylamine (50 mmol) and proceeding according to the abovementioned method C, 2-benzylaminomethylenecyclopentanone (7.4 g, efficiency: 70%) is produced in the form of a pale yellow powder.

Sources & evidence

ORD record: ord-0526842d28df44a4ab2d23484532fe5b
Source dataset: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08846125B2

Reaction notes

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