Benzylamine → HCID 89585460, compound

HRID 80336Notes

Reaction equation

HRID 80336 reaction equation
[Na].O[CH:3]=[C:4]1[CH2:9][CH2:8][CH2:7][O:6][C:5]1=[O:10].[CH2:11]([NH2:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([NH:18][CH:3]=[C:4]1[CH2:9][CH2:8][CH2:7][O:6][C:5]1=[O:10])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 895855013-Hydroxymethylenedihydropiran-2-one sodium salt

Product 1

HCID 89585460HCID 89585460, compoundYield 69%

Procedure

Using 3-hydroxymethylenedihydropiran-2-one sodium salt (50 mmol) and benzylamine (55 mmol) and proceeding according to the abovementioned method A1, 3-benzylaminomethylenetetrahydropiran-2-one (3.91 g, efficiency: 69%) is produced in the form of a white powder.

Sources & evidence

ORD record
ord-cd74fb2c511441e0a7834ac51a99672b
Source dataset
uspto-grants-2014_09
Patent number
US08846125B2

Reaction notes

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