HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → 4-(5-Phenylpyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 4-(5-Bromopyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 86649249 | — |
| Product | 4-(5-Phenylpyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 49869430 | — |
Reaction Steps
The title compound was prepared from the product of Example 65A and phenylboronic acid according to General Method B: 1H NMR (500 MHz, CDCl3) δ ppm 6 ppm 8.14 (d, 2 H), 7.56 (d, 2 H), 7.46 (t, 2 H), 7.39 (t, 1 H), 7.10 (s, 1 H), 3.73-3.37 (m, 5 H), 3.05-2.97 (m, 3 H), 2.27-2.17 (m, 4 H), 1.88-1.77 (m, 3 H); LC-MS Method D (ESI+) m/z 306.0 (M+H)+, retention time 1.28 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846661B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-599af1c2b56545d7a37f30bc44d1b743 |
| Source note | uspto-grants-2014_09 |