2-Methoxyphenylboronic acid → HCID 49869572, compound

HRID 80439Notes

Reaction equation

HRID 80439 reaction equation
Br[C:2]1[CH:3]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:5]=[N:6][CH:7]=1.[CH3:19][O:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1B(O)O>>[CH3:19][O:20][C:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[C:2]1[CH:3]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:5]=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 27339582-Methoxyphenylboronic acidHCID 866492494-(5-Bromopyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane

Product 1

HCID 49869572HCID 49869572, compound

Procedure

The title compound was prepared from the product of Example 65A and 2-methoxyphenylboronic acid according to General Method B: LC-MS Method D (ESI+) m/z 336.0 (M+H)+, retention time 1.30 minutes.

Sources & evidence

ORD record
ord-522b2c5bda664570be250938add78440
Source dataset
uspto-grants-2014_09
Patent number
US08846661B2

Reaction notes

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