HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dimethoxybenzeneboronic acid → 4-[5-(2,4-Dimethoxyphenyl)pyridin-3-yl]-1,4-diazatricyclo[4.3.1.13,8]undecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dimethoxybenzeneboronic acid | HCID 2734341 | — |
| Reactant | 4-(5-Bromopyridin-3-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 86649249 | — |
| Product | 4-[5-(2,4-Dimethoxyphenyl)pyridin-3-yl]-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 49869570 | — |
Reaction Steps
The title compound was prepared from the product of Example 65A and 2,4-dimethoxyphenylboronic acid according to General Method B: LC-MS Method D (ESI+) m/z 366.0 (M+H)+, retention time 1.37 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846661B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-779bfaa375434baab565828bf6124377 |
| Source note | uspto-grants-2014_09 |