HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethoxyphenylboronic acid → 4-[5-(2,5-Dimethoxyphenyl)-1,3-thiazol-2-yl]-1,4-diazatricyclo[4.3.1.13,8]undecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethoxyphenylboronic acid | HCID 2734342 | — |
| Reactant | 4-(5-Bromo-1,3-thiazol-2-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 86649262 | — |
| Product | 4-[5-(2,5-Dimethoxyphenyl)-1,3-thiazol-2-yl]-1,4-diazatricyclo[4.3.1.13,8]undecane | HCID 49869859 | — |
Reaction Steps
The title compound was prepared from the product of Example 105A and 2,5-dimethoxyphenylboronic acid according to General Method C: LC-MS Method D (ESI+) m/z 372.0 (M+H)+, retention time 1.44 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846661B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-adb5a21f4efc4adc8655a939b025af19 |
| Source note | uspto-grants-2014_09 |