HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 59548516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 66769548 | HCID 66769548 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59548516 | HCID 59548516 | — |
Reaction Steps
A mixture of Example 180C (29.4 g, 0.117 mol) and Raney®-nickel (30 g) in 2 L of methanol saturated with NH3 was stirred under H2 (50 psi) at 50° C. for 24 hours. After cooling and removal of the catalyst, the mixture was concentrated under reduced pressure to obtain the title compound which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08846663B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-b2c257b0f0d24de78212dd455e105606 |
| Source note | uspto-grants-2014_09 |