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HRID8066

反应详情

EQUATION

反应方程式

HRID 8066 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CCOC(=O)C(C(C)=O)C(C)=O
HCID79063

Ethyl 2-acetylacetoacetate

C8H12O4

结构：Cl.NNC1CCCCC1
HCID207836

Cyclohexylhydrazine--hydrogen chloride (1/1)

C6H15ClN2

PRODUCTS

生成物

1
结构：CCOC(=O)c1c(C)nn(C2CCCCC2)c1C
HCID9794939

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Similar to Example 1, equimolar amounts of cyclohexyl hydrazine hydrochloride and 2-acetyl-3-oxobutyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. Analysis confirmed synthesis of the named product (m.p. 66° C.–67° C.).