HRID8070

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID1049

Pyridine

C5H5N

HCID79063

Ethyl 2-acetylacetoacetate

C8H12O4

HCID2723914

(3-Fluorophenyl)hydrazine--hydrogen chloride (1/1)

C6H8ClFN2

PRODUCTS

生成物

HCID9856538

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Similar to Example 1, equimolar amounts of 3-fluorophenylhydrazine hydrochloride and 2-acetyl-3-oxo-butyric acid ethyl ester were combined in a solution of 50% pyridine in ethanol. Analysis showed that resulting solid was the named product (m.p. 55° C.–56.1° C.).

WORKUP

后处理

customthat resulting solid