Diethyl Ether → 2-(4-oxocyclohexyl)-2,3-dihydro-1H-isoindole-1,3-dione

HRID 807892Notes

Reaction equation

HRID 807892 reaction equation
[C:1]1(=[O:18])[c:2]2[c:3]([cH:14][cH:15][cH:16][cH:17]2)[C:4](=[O:13])[N:5]1[CH:6]1[CH2:7][CH2:8][CH:9]([OH:12])[CH2:10][CH2:11]1.[CH3:30][CH2:31][O:32][CH2:33][CH3:34].[Cl:35][CH2:36][Cl:37].[O:19]=[Cr:20]([Cl:21])([O-:22])=[O:23].[nH+:24]1[cH:25][cH:26][cH:27][cH:28][cH:29]1>>[C:1]1(=[O:18])[c:2]2[c:3]([cH:14][cH:15][cH:16][cH:17]2)[C:4](=[O:13])[N:5]1[CH:6]1[CH2:7][CH2:8][C:9](=[O:12])[CH2:10][CH2:11]1

Participants

6

Reactant 5

HCID 3283Diethyl EtherHCID 6344DichloromethaneHCID 288726trans-2-(4-Hydroxycyclohexyl)-isoindole-1,3-dioneHCID 4989215PyridiniumHCID 178418299HCID 178418299, compound

Product 1

HCID 119983912-(4-oxocyclohexyl)-2,3-dihydro-1H-isoindole-1,3-dione

Sources & evidence

ORD record
ord-90ddda43c5fa446283b32665eb6ba3c1
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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