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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 80921Generated: October 25, 2026

4-Aminophenylboronic acid → HCID 58006551, compound

https://huagongshe.com/reaction/80921

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Aminophenylboronic acidHCID 2734615—
Reactant4-(Tetramethyl-1,3,2-dioxaborolan-2-yl)anilineHCID 2734620—
Reactant1-(6-Chloro-pyridazin-3-yl)-4-isopropyl-perhydro-1,4-diazepineHCID 86637103—
ProductHCID 58006551HCID 58006551—

Reaction Steps

The title compound was prepared by a similar procedure to that described in Example 68, starting from 1-(6-chloro-pyridazin-3-yl)-4-isopropyl-perhydro-1,4-diazepine and 4-aminophenylboronic acid, pinacol cyclic ester. 1H NMR (400 MHz, CDCl3) δ 7.82 (d, 2H), 7.53 (d, 1H), 6.76 (m, 3H), 3.86 (t, 2H), 3.77 (m, 4H), 2.93 (heptet, 1H), 2.81 (m, 2H), 2.58 (m, 2H), 1.95 (m, 2H), 1.00 (d, 6H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08846677B2
Source datasetuspto-grants-2014_09
ORD IDord-75931463580e41bd961246eaa1f9d431
Source noteuspto-grants-2014_09