Methanol → 3-tert-butyl-5-iodosalicylaldehyde

HRID 810001Notes

Reaction equation

HRID 810001 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[c:5]1[c:6]([OH:13])[c:7]([CH:8]=[O:9])[cH:10][cH:11][cH:12]1.[CH2:22]([N+:23]([CH3:24])([CH3:25])[CH3:26])[c:27]1[cH:28][cH:29][cH:30][cH:31][cH:32]1.[CH2:36]([Cl:37])[Cl:38].[CH3:34][OH:35].[I:14]([Cl:15])(=[O:16])=[O:17].[I:18]([Cl:19])(=[O:20])=[O:21].[OH2:33]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[c:5]1[c:6]([OH:13])[c:7]([CH:8]=[O:9])[cH:10][c:11]([I:14])[cH:12]1

Participants

7

Reactant 6

HCID 887MethanolHCID 962WaterHCID 5964BenzyltrimethylammoniumHCID 6344DichloromethaneHCID 36786753-tert-Butyl-2-hydroxybenzaldehydeHCID 56924452CID 569244522×

Product 1

HCID 120345043-tert-butyl-5-iodosalicylaldehyde

Sources & evidence

ORD record
ord-50e535edda224871929b9e165aa3fb23
Source dataset
Test data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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